Lim, Y. W.; Ong, M. J. H.; Hewitt, R. J., Improved synthesis of glucosinolates. Synthesis 2018, 50 (8), 1640-1650.
Abstract:
Herein we describe an improved synthesis of glucosinolates, in which the quantity and cost of materials have been reduced by approximately an order of magnitude compared to typical literature procedures. This allowed us to produce multiple glucosinolates in 10–25 gram batches using vessel sizes no larger than 0.5 litres.
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Funding Info:
This work was supported by the Institute of Chemical and Engineering Sciences, Agency for Science, Technology and Research (A*STAR), Singapore (ICES/14-3E5A02 and ICES/15-1E5A06).